An Introductory Course of Quantitative Chemical Analysis With Explanatory Notes

About this eBook

Author

Talbot, Henry Paul, 1864-1927

Credits

Produced by Kevin Handy, Dave Maddock, Josephine Paolucci and the Online Distributed Proofreading Team

Language

English

LoC Class

QD: Science: Chemistry

Subject

Chemistry, Analytic -- Quantitative

Category

Text

eBook-No.

12787

Project Gutenberg

https://www.gutenberg.org/ebooks/12787

Release Date

June 30, 2004

Copyright

Public domain in the USA.

Contents

1. 1.AN INTRODUCTORY COURSE — BY
2. 2.PREFACE
3. 3.CONTENTS — PART I. INTRODUCTION — PART II. VOLUMETRIC ANALYSIS — PART III. GRAVIMETRIC ANALYSIS
4. 4.PART I
5. 5.GENERAL DIRECTIONS — ACCURACY AND ECONOMY OF TIME — NOTEBOOKS — REAGENTS — WASH-BOTTLES — TRANSFER OF LIQUIDS — EVAPORATION OF LIQUIDS
6. 6.PART II — MEASURING INSTRUMENTS — THE ANALYTICAL BALANCE — WEIGHTS — BURETTES — PREPARATION OF A BURETTE FOR USE — READING OF A BURETTE — CALIBRATION OF GLASS MEASURING DEVICES — CALIBRATION OF THE BURETTES — PIPETTES — CALIBRATION OF PIPETTES — FLASKS — GRADUATION OF FLASKS
7. 7.GENERAL DIRECTIONS FOR VOLUMETRIC ANALYSES — STANDARD SOLUTIONS — NORMAL SOLUTIONS
8. 8.I. NEUTRALIZATION METHODS
9. 9.GENERAL DISCUSSION — INDICATORS — BEHAVIOR OF ORGANIC INDICATORS — PREPARATION OF INDICATOR SOLUTIONS — PREPARATION OF STANDARD SOLUTIONS — COMPARISON OF ACID AND ALKALI SOLUTIONS
10. 10.STANDARDIZATION OF HYDROCHLORIC ACID — STANDARDIZATION
11. 11.DETERMINATION OF THE TOTAL ALKALINE STRENGTH OF SODA ASH
12. 12.DETERMINATION OF THE ACID STRENGTH OF OXALIC ACID
13. 13.II. OXIDATION PROCESSES
14. 14.BICHROMATE PROCESS FOR THE DETERMINATION OF IRON — NORMAL SOLUTIONS OF OXIDIZING OR REDUCING AGENTS — PREPARATION OF SOLUTIONS — INDICATOR SOLUTION — COMPARISON OF OXIDIZING AND REDUCING SOLUTIONS — STANDARDIZATION OF POTASSIUM BICHROMATE SOLUTIONS — STANDARDIZATION
15. 15.DETERMINATION OF IRON IN LIMONITE
16. 16.DETERMINATION OF CHROMIUM IN CHROME IRON ORE
17. 17.PERMANGANATE PROCESS FOR THE DETERMINATION OF IRON — PREPARATION OF A STANDARD SOLUTION — COMPARISON OF PERMANGANATE AND FERROUS SOLUTIONS — STANDARDIZATION OF A POTASSIUM PERMANGANATE SOLUTION — STANDARDIZATION
18. 18.DETERMINATION OF IRON IN LIMONITE
19. 19.DETERMINATION OF THE OXIDIZING POWER OF PYROLUSITE
20. 20.IODIMETRY — PREPARATION OF STANDARD SOLUTIONS — INDICATOR SOLUTION — COMPARISON OF IODINE AND THIOSULPHATE SOLUTIONS — STANDARDIZATION OF SOLUTIONS
21. 21.DETERMINATION OF COPPER IN ORES
22. 22.DETERMINATION OF ANTIMONY IN STIBNITE
23. 23.CHLORIMETRY
24. 24.DETERMINATION OF THE AVAILABLE CHLORINE IN BLEACHING POWDER
25. 25.DETERMINATION OF SILVER BY THE THIOCYANATE PROCESS — STANDARDIZATION — DETERMINATION OF SILVER IN COIN
26. 26.PART III
27. 27.GENERAL DIRECTIONS — PRECIPITATION — FUNNELS AND FILTERS — FILTRATION AND WASHING OF PRECIPITATES — DESICCATORS — CRUCIBLES — PREPARATION OF CRUCIBLES FOR USE — IGNITION OF PRECIPITATES
28. 28.DETERMINATION OF CHLORINE IN SODIUM CHLORIDE
29. 29.DETERMINATION OF IRON AND OF SULPHUR IN FERROUS AMMONIUM SULPHATE, — DETERMINATION OF IRON
30. 30.DETERMINATION OF SULPHUR
31. 31.DETERMINATION OF SULPHUR IN BARIUM SULPHATE
32. 32.DETERMINATION OF PHOSPHORIC ANHYDRIDE IN APATITE — PRECIPITATION OF AMMONIUM PHOSPHOMOLYBDATE — PRECIPITATION OF MAGNESIUM AMMONIUM PHOSPHATE — REPRECIPITATION AND IGNITION OF MAGNESIUM AMMONIUM PHOSPHATE
33. 33.ANALYSIS OF LIMESTONE — DETERMINATION OF MOISTURE
34. 34.DETERMINATION OF FERRIC OXIDE AND ALUMINIUM OXIDE (WITH MANGANESE)
35. 35.DETERMINATION OF CALCIUM
36. 36.DETERMINATION OF MAGNESIUM
37. 37.DETERMINATION OF CARBON DIOXIDE
38. 38.DETERMINATION OF LEAD, COPPER, IRON, AND ZINC IN BRASS
39. 39.DETERMINATION OF COPPER AND LEAD
40. 40.DETERMINATION OF IRON
41. 41.DETERMINATION OF ZINC
42. 42.DETERMINATION OF SILICA IN SILICATES — PREPARATION OF THE SAMPLE — FUSION AND SOLUTION — DEHYDRATION AND FILTRATION — IGNITION AND TESTING OF SILICA
43. 43.PART IV
44. 44.PROBLEMS — VOLUMETRIC ANALYSIS — GRAVIMETRIC ANALYSIS
45. 45.APPENDIX — ELECTROLYTIC DISSOCIATION THEORY — THE FOLDING OF A FILTER PAPER — !SAMPLE PAGES FOR LABORATORY RECORDS! — STRENGTH OF REAGENTS — CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS — INTERNATIONAL ATOMIC WEIGHTS
46. 46.INDEX

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